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When working with lye, please wear goggles or a full-face visor (an industrial face protector), neoprene gloves, and a PVC lab apron.  

The goal is to get the precipitate between pH 8.5 and 10.78. After you get the precipitate, the goal is to wash it well. Washing the precipitate will take the pH down closer to 8.5. The m-state is in the precipitate. You can take the pH down to 4 or 5 and the washed precipitate will re-dissolve but the m-state will still be in the liquid. 

Approximately two teaspoons of granulated NaOH in nine (9) ounces of distilled water. 

I diluted 2 spoons of Pure Lye Crystals in one liter of distilled water, 

remember: ADD ACID TO WATER, NEVER ADD WATER TO ACID). 

Dissolve 125 grams of sodium hydroxide in 1 liter of water. Do this slowly, adding only a tablespoon while stirring and waiting for it to dissolve before adding the next tablespoon. 

 
 
 
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